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The Use of Amino Acid L-Prolineas Catalyst forDirect Asymmetric Aldol Reactions
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001
AA00002431_00001
005
20210622151224.0
006
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210622n^^^^^^^^xx^^^^^^s^^^^^^^^^^^eng^d
245
00
|a
The Use of Amino Acid L-Prolineas Catalyst forDirect Asymmetric Aldol Reactions
|h
[electronic resource].
260
|a
Edison, NJ :
|b
Middlesex College,
|c
2014 December 8.
490
|a
Student Symposium 2014.
520
3
|a
I have explored the asymmetric aldol reaction using natural amino acid L-proline as the catalyst. Amino acid L-Proline mimics class I aldolase enzyme to drive the aldol reaction through enamine-based mechanism. The use of catalyst L-Proline is the first example of amine-based asymmetric class I aldolase mimics. In the first part of this project, weexplored the direct asymmetric aldol reaction between acetone and 4-nitrobenzaldehyde in the presence of 30 mol % of L-proline.The reaction was set at room temperature under normal condition, and we got 2 products: aldol and α,β-unsaturated ketone product. Detail characterization of the two products was done using TLC, Column Chromatography, NMR and IR. The percent yield of asymmetric aldol product was 70% which is comparable to the published value of 68%. The yield of α,β-unsaturated ketone was10.5%. Further in the project, we explored the same aldol reaction using p-Anisaldehyde in place of 4-nitrobenzaldehyde. Only one product was obtained, and the exclusive product was α,β-unsaturated ketone instead of the expected asymmetric aldol product
533
|a
Electronic reproduction.
|c
Middlesex County College Institution,
|d
2021.
|f
(Middlesex County College)
|n
Mode of access: World Wide Web.
|n
System requirements: Internet connectivity; Web browser software.
535
1
|a
Middlesex County College Institution.
648
|a
2014-2015
|y
Academic Year 2014-2015.
650
0
|a
College students -- poster presentations.
650
0
|a
Student Works -- Natural Sciences -- poster presentations.
650
0
|a
Chemistry.
650
0
|a
Student works -- Natural Sciences -- academic theses.
650
|a
Middlesex College (Edison, NJ) -- Student works.
650
0
|a
Middlesex County College (Edison, NJ).
700
1
|a
Tran, Tram,
|e
author, primary.
700
1
|a
Ghosh, Phalguni,
|e
advisor.
700
|a
Middlesex College, Department of Natural Sciences.
|4
spn
830
0
|a
Middlesex County College.
830
0
|a
Student Symposium.
830
0
|a
Student Works.
852
|a
MCC
|c
Student Symposium
856
40
|u
http://middlesexcc.sobeklibrary.com/AA00002431/00001
|y
Electronic Resource
992
04
|a
https:/digital.middlesexcc.edu/content/AA/00/00/24/31/00001/Research Thesis - Tram Tran--12-18-2014thm.jpg
997
|a
Student Symposium
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